Supporting Information (SI)
نویسنده
چکیده
Nanorod Synthesis. 0.21g of CdO, 1.08 g of ODPA and 2.73 g of TOPO were loaded into a 25 ml three-neck flask and heated to 110 °C under Argas flow at which ODPA and TOPO were dissolved (mixture becomes a brown colour). The mixture is degassed at 110°C for 30 minutes followed by switching from gas to vacuum line with a vacuum range of 150-200 mTorr. The mixture is heated to 300°C under Ar-gas at which CdO completely dissolves and the solution becomes clear. The Mixture is is cooled to 110°C and further degassed for another 30 minutes under similar vacuum range (150-200 mTorr). After this second degas, the apparatus is switched back to Ar-gas line and mixture was heated to 300°C at which 0.8 g of Sulphur stock solution (0.65 g of Sulphur powder dissolved in 8.25 g of TOP) was injected. After injection, nanocrystals grew at 300°C for 30 minutes to reach desired size.
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